Additionally, this notice proposes that no threshold be established for domestic and international transactions. The Drug Enforcement Administration (DEA) has determined that these controls are necessary to prevent the diversion of these chemicals to clandestine drug laboratories. Nonetheless, it is likely that chemical distributors do maintain records of shipments and customers even if shipping papers are not required. The white form is extremely flammable and toxic and must be stored and shipped in water. What Specific Chemicals Does This Proposed Regulation Include? One of the two producers recently acquired the other. White phosphorus is primarily used to produce phosphoric acid and other phosphorus compounds including phosphorus trichloride and phosphorous pentasulfide and phosphorus pentoxide. crystalline) forms (white, red and black). Each customer appears to be a large industrial firm. Phosphorus is also subject to Department of Transportation (DOT) hazardous material ("hazmat") regulations so that interstate and intrastate transportation require shipping papers. Sodium hypophosphite decomposes into phosphine which is highly irritating to the respiratory tract and disodium phosphate. In case of eye contact Flush eyes with water as a precaution. How Many Importers and Exporters Are Potentially Affected? Therefore, use of these alternate methods poses increased hazards for both law enforcement and for the public. Notice of Registration, Program Description The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The Idaho State Police, however, have closely monitored the illicit use of white phosphorus. Sodium hypophosphite monohydrate 10039-56-2 . Handlers which acquire phosphorus and convert it to non-regulated forms will not be subject to CSA regulatory requirements. DEA believes that the use of white phosphorus is under-reported. Since laboratory seizure data sparked concerns over the illicit use of white phosphorus and hypophosphorous acid, the DEA broadened the scope of its research to include the entire phosphorus chemical industry. Comments must be submitted on or before November 24, 2000. H2O. *           *          *           *         *. Why Does DEA Believe That This Regulation Will Not Impose a Significant Burden on a Substantially Large Number of Firms? Fire Extinguishing Media: Use any means suitable for extinguishing surrounding fire. The formula for this acid is generally written H 3 PO 2, but a more descriptive presentation is HOP(O)H 2, which highlights its monoprotic character. Drug Traffic Control, Reporting and Recordkeeping Requirements. Significant Guidance Documents DEA obtained 1998 and 1999 sales data from both producers. Over a two-year period, the two firms had only a few customers. The sodium hypophosphite market is expected to grow because of its increased demand from various end-use … In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. Ungraded products supplied by Sigma Aldrich are The TRI data have the advantage that they provide information on the quantity of a chemical transferred offsite as a waste, and the name of the offsite treatment facility. A few reported releasing the substance to publicly owned treatment works (i.e., wastewater treatment). Salts of hypophosphorous acid are known as hypophosphite salts. View detailed Import data, price, monthly trends, major importing countries, major ports of sodium hypophosphite under HS Code 2835 00-24553 Filed 9-22-00; 8:45 am] Therefore, this action has not been reviewed by the Office of Management and Budget. Safety Data Sheet (Sodium Hypophosphite Solution) DATE PREPARED: 7/28/2015 Page 6 of 6 California Prop. A limited number of other facilities manufacture phosphorus as a by-product or import phosphorus. The majority of clandestine methamphetamine laboratories seized in the U.S. utilize phosphorus chemicals as catalysts to drive the chemical conversion of ephedrine or pseudoephedrine to methamphetamine. New Sodium Hypophosphite products manufacturing in China, with stylish and cool design emerge. While the manganese salt is used primarily in nylon fiber production, it also has application as a chemical intermediate. Based on analysis of chemistry and actual illicit use, DEA finds that these three chemicals are important to the manufacture of methamphetamine and therefore meet the definition of List I chemicals. Reports Required by 21 CFR If not confined within the reaction vessel, ingestion of this poisonous gas can result in death. (37) Iodine or tincture of iodine. SDS; Sodium hypophosphite monohydrate. Given our expertise spanning more than 55 years, it is the best quality product of its kind on the market. What Steps Has the DEA Taken To Solicit Information From the Legitimate Phosphorus Industry? The resulting nickel deposit contains up to 15% phosphorus. [2] The latter requires that the substrate is activated with fine particles of palladium. Chemical mixtures for these applications are formulated within a range of less than one percent to no greater than 20 percent in sodium hypophosphite. 5 min read . SODIUM HYPOPHOSPHITE (MONOHYDRATE) AR is not on the REACH Candidate List SODIUM HYPOPHOSPHITE (MONOHYDRATE) AR is not on the REACH Annex XIV List 15.1.2. [[Page 57578]] What Is Phosphorus Used for and How Large Is the Industry? Based on the chemical composition of this product it is assumed that the mixture can be treated in an acclimatized biological … The DEA has also noted that detailed recipes describing the production of methamphetamine (using red phosphorus, white phosphorus and hypophosphorous acid) are being disseminated on the Internet. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. Most of these companies would not be required to register with DEA unless they sell phosphorus or transfer it offsite. Many of the transfers were for recovery or recycling and a few were for disposal in landfills. phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) EC Number: 600-090-7 CAS Number: 10039-56-2 Molecular formula: NaH4PO3 IUPAC Name: phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) DATES: Written comments must be submitted on or before November 24, 2000. It is soluble in water, and easily absorbs moisture from the air. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. H 2 O. EUR. It is also prepared as colorless, pearly crystalline plates. English-Tamil dictionary. Global Sodium Hypophosphite Market. 65 Components: This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm Section 16. Sodium hypophosphite is the most commercially available salt and is distributed in a white crystalline form. Since no industry input was received in response to the Advance Notice of Proposed Rulemaking, DEA directly contacted domestic producers of elemental phosphorus and importers of phosphorus chemicals. Industrial uses of red phosphorus include the manufacture of pyrotechnics, safety matches, phosphoric acid and other phosphorus compounds, fertilizers, incendiary shells, smoke bombs, tracer bullets, and pesticides. It also maintains List I of chemicals and List II of chemicals, which contain chemicals which are used to manufacture the controlled substances/illicit drugs. The analysis identified two main producers of the hypophosphites. El-Ahraf A, Van Willis W, Vinjamoori DV. sodium hypophosphite. Environmental Toxicity: No information found. SODIUM HYPOPHOSPHITE … Sodium Hypophosphate; sodium hyposulfate; Look at other dictionaries: that they are not covered by the DOT hazmat rules. Sodium Hypophosphite (DEA List I Chemical), Crystal, Reagent This item is a DEA LIST 1 CHEMICAL + CALIFORNIA DOJ PRECURSOR. Customer Service Plan Very small volumes are used to produce ultra-high-purity phosphorus semiconductor grades) for application in the electronics industry. Flame Retardant – Sodium Hypophosphite may be used as a partial fire retardant. Chemical Control Program H 2 O. [Proposed Rules] This rule is not a major rule as defined by Section 804 of the Small Business Regulatory Enforcement Fairness Act of 1996. Publications & Manuals (27) Hypophosphorous acid and its salts (including ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite manganese hypophosphite magnesium hypophosphite and sodium hypophosphite 6797 (28) N-phenethyl-4-piperidone (NPP) 8332 (29) Iodine 6699 (30) Ergocristine and its salts 8612 (b) List II chemicals: Additionally, hypophosphorous acid is covered in interstate commerce. Phosphorus is covered by the Toxic Release Inventory (TRI) program, which requires an annual report to EPA listing the maximum quantity on site, the uses of the chemical, releases to the environment, and transfers offsite. Drug Disposal InformationDrug and Chemical Information It is common to find 500 ml bottles of hypophosphorous acid or multi-ounce quantities of red phosphorus repackaged in unlabeled bags at seized laboratories. The Deputy Administrator further certifies that this rulemaking has been drafted in accordance with the principles in Executive Order 12866 section 1(b). DEA also examined Environmental Protection Agency (EPA) reporting requirements pertaining to phosphorus, hypophosphorous acid, and the hypophosphites. In case of eye contact Flush eyes with water as a precaution. This rule will not result in the expenditure by state, local, and tribal governments, in the aggregate, or by the private sector, of $100,000,000 or more in any one year, and will not significantly or uniquely affect small governments. In an effort to better estimate the potential impact of this proposed action, the DEA conducted an analysis of various data sources relating to the manufacture, distribution, and use of phosphorus, hypophosphorous acid, and the hypophosphites. REGULATIONS.GOV, DOJ Legal Policies and Disclaimers    |    DOJ Privacy Policy    |    FOIA    |    Section 508 Accessibility. Both quantitative and qualitative data were invited. BILLING CODE 4410-09-P. NOTICE: This is an unofficial version. For reasons set out above, it is proposed that 21 CFR Part 1310 be amended as follows: 1. What Related Chemicals Will Not Be Subject to This Control Action? It is a solid at room temperature, appearing as odorless white crystals. A thermal explosion will occur if sodium hypophosphite is heated under confinement. Ecological Information Environmental Fate: No information found. DEA has not been able to identify any household uses for red phosphorus, white phosphorus or hypophosphorous acid and its salts. 2 NaPO 2 H 2 → PH 3 + Na 2 HPO 4. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. The hypophosphorous acid method is also extremely hazardous since it produces phosphine gas. It is soluble in water, and easily absorbs moisture from the air. Non-California customers must complete form QAF482. This would be an undesired consequence, since both the white phosphorus and hypophosphorous acid methods of illicit methamphetamine production are significantly more hazardous methods. The CSA, therefore, provides the Attorney General with authority to establish a threshold amount for "listed chemicals" if the Attorney General so elects. COVID-19 Information CMEA (Combat Meth Epidemic Act) If you have suggestions as to how to improve the clarity of this regulation, call or write Patricia M. Good, Chief, Liaison and Policy Section, Office of Diversion Control, Drug Enforcement Administration, Washington, DC 20537, telephone (202) 307-7297. DEA has identified only two domestic producers of white phosphorus. Sodium Hypophosphite (Monohydrate) CAS No 10039-56-2 MATERIAL SAFETY DATA SHEET SDS/MSDS . The sodium salt is used primarily in electroless nickel plating. The DEA did receive six comments from law enforcement entities and two comments from Federal prosecutors in support of the control of red phosphorus as a listed chemical. Many forensic laboratories do not differentiate samples as being white versus red phosphorus. Because of their use and importance in the illicit manufacture of methamphetamine, a Schedule II controlled substance, the DEA is proposing the addition of red phosphorus, white phosphorus (also known as yellow phosphorus) and hypophosphorous acid (and its salts) as List I chemicals. Other forms of phosphorus and other phosphorus chemicals are manufactured from white phosphorus. The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The trend continues into calendar year 2000. As Part of This Proposed Rulemaking, the DEA Again Invites Input Regarding the Legitimate Uses for These Chemicals. H2O. Their information indicates that in southeastern Idaho, white phosphorus is frequently encountered in methamphetamine laboratories. It is a solid at room temperature, appearing as odorless white crystals. Physical. Therefore, this proposed regulation will only affect the distribution of less than 2% of the industry at the end user level. 12. It is soluble in water, and easily absorbs moisture from the air. Global Sodium Hypophosphite Market was valued US$ XX Mn in 2019 and is expected to reach US$ 975.12 Mn by 2026, at a CAGR of around XX % during a forecast period.. Chemical compounds that contain the hypophosphite ions are called hypophosphites. Sodium hypophosphite is a colorless hygroscopic solid, soluble in water. QAF482 Designation of Authorized Purchaser: DEA List 1 & 2 Chemicals QAF481 … Interpretation Translation Additionally, two producers of hypophosphorous acid were identified. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. Sodium Hypophosphite (Monohydrate) CAS No 10039-56-2 MATERIAL SAFETY DATA SHEET SDS/MSDS . While the vast majority of these laboratories utilized red phosphorus, DEA is aware that a number of seized laboratories have used white phosphorus. DEA has determined that this is not a significant rulemaking action. 4.2 Most important symptoms and effects, both acute and delayed To the best of our knowledge, the chemical, physical, and toxicological properties … Medical Missions The United States Drug Enforcement Administration designated sodium hypophosphite as a List I chemical under 21 CFR 1310.02 effective November 17, 2001, specifically mentioning the compound together with several other salts of hypophosphorous acid. Other forms of phosphorus and … In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. Contact most popular products of manufacturers, trading companies, wholesalers & exporter directly on Made-in-China.com Rinse mouth with water. All transactions in those substances are subject to the reporting requirements. The United States Drug Enforcement Administration (DEA) maintains lists regarding not only the classification of illicit drugs (see DEA Schedules). (ii) Red phosphorus Ion Exchange Resin – It will provide a source of electrons in resin regeneration. Find here Sodium Hypophosphite manufacturers & OEM manufacturers India. Red phosphorus is usually prepared as a powder and is more stable and less toxic than the white form. Since catalysts are necessary for the preferred method used by illicit laboratory operators, these phosphorus chemicals are important to the production of methamphetamine. [FR Doc. Given the small quantities and limited uses of these chemicals necessary for the production of methamphetamine, the DEA is proposing that no threshold be established for domestic and international transactions. (26) White phosphorus (Other names: Yellow Phosphorus)--6796 Rinse mouth with water. The DEA has identified two manufacturers of sodium hypophosphite in the United States. Sodium Hypophosphite Hydrate (DEA List I Chemical), also known as sodium phosphinate, is used for electroless nickel plating. Registrant Record of Controlled Substances Destroyed Sodium hypophosphite (NaPO 2 H 2) is the sodium salt of hypophosphorous acid. Black phosphorus and phosphate rock will not be affected by this proposed action. White phosphorus is much more flammable and toxic than red phosphorus. 243663 ; Sigma-Aldrich pricing. Sodium hypophosphite is mainly used for electroless nickel plating (Ni-P). DEA's research indicates that there are currently only two domestic producers of elemental phosphorus. Examples of these salts include: Ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite and sodium hypophosphite. Identifiers CAS Number. 822 and 823 and 21 CFR part 1309. Ungraded products supplied by Sigma Aldrich are. California customers must complete form QAF481 and be advised that there is a mandatory 21-day hold prior to shipment. Hypophosphorous acid is also used as a chemical intermediate in organic syntheses and as a polymerization and polycondensation catalyst. (28) Hypophosphorous acid and its salts (Including ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite and sodium hypophosphite) 6797 (29) N-phenethyl-4-piperidone (NPP) 8332 (30) Iodine: 6699 (31) Ergocristine and its salts: 8612 It also can be used as a food additive. as red phosphorus or white phosphorus) or used to produce all other phosphorus chemicals including sodium hypophosphite and hypophosphorous acid. The most abundant variety produced is white phosphorus (also known as yellow phosphorus). The second crystalline form is red phosphorus. This notice proposes, therefore, that no threshold be established for domestic and international transactions. Sodium hypophosphite is capable of reducing nickel ions in solution to metallic nickel on metal substrates as well as on plastic substrates. CMEA Required Training & Self-Certification, CSOS (Controlled Substances Ordering System), Registrant Record of Controlled Substances Destroyed, Regulated Machines (Tableting and Encapsulating). The MSDSs located for the hypophosphites indicate. The DEA reviewed independent data for 1997 indicating that approximately 250,000 metric tons of elemental phosphorus were consumed in the U.S. DEA's research indicates that there are currently only two domestic producers of elemental phosphorus. The hypophosphites are similarly produced by very few facilities. Therefore, the manufacture of methamphetamine requires only small quantities of these chemicals. Sodium Hypophosphite is used in formulating many pharmaceutical products. Sodium Hypophosphite Certificate of Analysis (COA) Product Name: Sodium Hypophosphite, Mono. While chemical mixtures are currently exempt from CSA chemical regulatory requirements, the DEA is preparing regulations pertaining to such mixtures. DEA Forms & Applications As List I chemicals, red phosphorus, white phosphorus, and hypophosphorous acid and its salts will become subject to the chemical regulatory control provisions and civil and criminal sanctions of the CSA. In 1998, 53 facilities reported to EPA for phosphorus. Handlers of these chemicals will also be required to maintain records and meet CSA import/export notification requirements for "regulated transactions" of these chemicals. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. The remaining 2% of the phosphorus (used domestically) is utilized in its elemental form (i.e. The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. Sodium Hypophosphite Monohydrate 10039-56-2 99.5-100 Not established Not established The anhydrous form of Sodium Hypophosphite has a CAS Number of 7681-53-0 [Phosphinic acid, sodium salt (1:1)] SECTION 4: FIRST AID MEASURES Inhalation: Remove affected person to fresh air; if symptoms persist seek medical attention. red phosphorus, white phosphorus and hypophosphorous acid and its salts.) Sodium Hypophosphite Monohydrate 10039-56-2 231-669-9 7640mg / kg Oral - rat Not established SECTION 12: ECOLOGICAL INFORMATION 12.1 No data are available on the adverse effects of this material on the environment. (1) * * * 13. Sodium Hypophosphite Hydrate (DEA List I Chemical), also known as sodium phosphinate, is used for electroless nickel plating. If swallowed Never give anything by mouth to an unconscious person. Year-End Reports, Cases Against Doctors Hypophosphorous acid (HPA), or phosphinic acid, is a phosphorus oxyacid and a powerful reducing agent with molecular formula H 3 PO 2.It is a colorless low-melting compound, which is soluble in water, dioxane, and alcohols. Medical Chinese dictionary (湘雅医学词典). Expect a visit eventually from the DEA if you sign for any amount at all. It is a solid at room temperature, appearing as odorless white crystals. With this method, a durable nickel-phosphorus film can coat objects with irregular surfaces, and can widely be used ionics, aviation and the petroleum field. Therefore, DEA has sought information on the phosphorus chemical trade so that diversion of these chemicals may be prevented with minimal impact on legitimate industry. The authority citation for part 1310 continues to read as follows: 2. 601 et seq.). A turnkey product, we offer sodium hypophosphite under the form of ready-to-use solution. RESOURCES > Federal Register Notices > Rules - 2000 > Control of Red Phosphorus, White Phosphorus and Hypophosphorous Acid (and Its Salts) as List I Chemicals, [Federal Register: September 25, 2000 (Volume 65, Number 186)] Meetings & EventsWhat's New, ARCOSBCM Online Pricing & More Info SODIUM HYPOPHOSPHITE-1-HYDRATE, R. G., RE AGPH. If red phosphorus alone is controlled, DEA has concluded that clandestine laboratory operators would rapidly move to white phosphorus and hypophosphorous acid. This action has been analyzed in accordance with the principles and criteria in Executive Order 13132, and it has been determined that this rule does not have sufficient federalism implications to warrant the preparation of a Federalism Assessment. Additionally, a review of calendar years 1998-1999 clandestine laboratory seizure data (reported by the El Paso Intelligence Center and the Western States Information Network) indicated that more than 3750 seized methamphetamine laboratories were confirmed as utilizing phosphorus. Palm's SHP is blended exclusively from high purity SHP for use in electroless nickel solutions. Why Does DEA Believe That Control of Red Phosphorus, White Phosphorus, and Hypophosphorous Acid (and its Salts) Is Necessary? Its assay is 810g/L, meaning a 60% solution. Of the three chemicals subject to this proposed rule, only phosphorus is regulated under programs that require reporting to EPA. The DEA is proposing that the white and red forms of elemental phosphorus be designated as List I chemicals. Om inget annat anges ges data för material i deras standardtillstånd (vid 25 ° C, 77 kF). It will not have a significant economic impact on a substantial number of small business entities. This included an analysis of current chemical producers and marketing directories (to identify companies listing themselves as sources of these chemicals). It is also used as a reducing agent, analytical reagent, polymerization catalyst, polymer stabilizer, and fire retardant. One mission of the DEA and the CA-DOJ is to disrupt the illicit production of controlled substances by preventing diversion of precursor chemicals. It also has applications as a reducing agent and as an antioxidant. 1272/2008 [CLP] Extra labelling to displayExtra classification(s) to display The DEA did not receive any comments or input from the phosphorus industry in response to this Notice. It decomposes into phosphine which is irritating to the respiratory tract and disodium phosphate. A review of chemical marketing directories identified at least 39 companies, other than the manufacturers, that claim to sell these substances. DATA Waived Physicians Most consumers are large entities, which primarily use elemental phosphorous in the manufacture of phosphorous chemicals not impacted by this proposed regulation. Prior to preparing this proposal the DEA also solicited information directly from importers. A review of the 50 largest methamphetamine laboratories seized by DEA in 1998 was recently conducted. This search engine indexes the Drug Enforcement Administration Diversion Control Program Web Site (www.deadiversion.usdoj.gov) only. While hypophosphorous acid (H3PO2) is most commonly sold as 10%, 30% or 50% solutions, the DEA is proposing the control of all aqueous dilutions of hypophosphorous acid. In addition, Material Safety Data Sheets (MSDSs) were collected. • Hydrogen donor in the enantioselective transfer hydrogenation of aliphatic and aromatic ketones to corresponding alcohols in presence of ruthenium catalyst. [DOCID:fr25se00-25], Control of Red Phosphorus, White Phosphorus and Hypophosphorous Acid (and Its Salts) as List I Chemicals. H2O. Non-California customers must complete form QAF482. Additionally, it is likely that the CSA recordkeeping requirements are already being met as part of normal business practice. Quota Applications If not stored in a solution, white phosphorus spontaneously combusts. what is sodium hypophosphite used for. It is a critical ingredient of electroless nickel plating solutions. The Department of Justice does not endorse the organizations or views represented by this site and takes no responsibility for, and exercises no control over, the accuracy, accessibility, copyright or trademark compliance or legality of the material contained on this site. Can result in death hypophosphite … sodium hypophosphite should be kept in a crystalline! Primarily used to produce ultra-high-purity phosphorus semiconductor grades ) for application in the form white. 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